TECHNOLOGY FOCUS - ELECTRICAL POWER AND ENERGY - Preferred Process: A lithium secondary battery is formed by forming cathode with electrochemical activity, an anode having an active material layer and a separation film comprising an electrolyte provided between cathode and anode.    TECHNOLOGY FOCUS - INORGANIC CHEMISTRY - Preferred Compound: The transition metal alloy is of formula: AxB'y. The transition metal oxide is of formula: GOz. The active material layer of anode contains lithium compound of formula: LiEiFjG(1-i-j) or LiFeiD'(1-i)PO4.A=silicon, tin, aluminum, germanium, gallium, indium, antimony, lead, bismuth, magnesium or zinc;B'=copper, nickel, cobalt, iron, manganese, chromium, vanadium, titanium, scandium, molybdenum, ruthenium or tungsten;x,y=greater than 0 and less than or equal to 1;G=scandium, titanium, vanadium, chromium, manganese, iron, cobalt, nickel, copper, molybdenum, tungsten, ruthenium or zirconium;z=greater than 0 and less than or equal to 3;E,F,G=chromium, manganese, iron, cobalt or nickel;D'=titanium, vanadium, chromium, manganese, iron, cobalt, nickel or copper;andi,j=0-1.Preferred Process: The electrode has a current collection layer formed using a material (a) of copper, nickel, cobalt, iron, manganese, chromium, vanadium, titanium, scandium, molybdenum, ruthenium and/or tungsten, and/or a material (b) of silicon, tin, aluminum, germanium, gallium, indium, antimony, lead, bismuth, magnesium and/or zinc and heating material (a) and/or material (b). A slurry containing transition metal alloy or transition metal oxide, a conductive material, a binder resin and a solvent is coated to a metal current collection component to form electrode having phase with electrochemical activity. A copper-indium alloy is charged at 50-200 degrees C and discharged at 10-30 degrees C to obtain cathode. Preferred Composition: The electrolyte contains an organic solvent and a lithium salt such as lithium(bis)oxaloborate, lithium(bis)trifluoroethanesulfonimide, lithium bis(pentafluoroethylsulfonyl)imide, lithium perchlorate, lithium trifluoromethanesulfonate, lithium hexafluoroarsenate, lithium tetrafluoroborate and lithium bis(trifluoromethanesulfonimide), lithium hexafluorophosphate, lithium thiocyanate and/or lithium trifluoromethanesulfonemethide.    TECHNOLOGY FOCUS - ORGANIC CHEMISTRY - Preferred Compound: The organic solvent is ethylene carbonate, propylene carbonate, diethyl carbonate, 1,2-dimethoxyethane, 1,2-diethoxyethane, gamma -butyrolactone, tetrahydrofuran, 2-methyltetrahydrofuran, 1,3-dioxolane, 4-methyl-1,3-dioxolane, diethylether, sulfolane or polyethylene oxide.