NOVELTY - Recycling organic chlorides from distillation residue of methane chloride and/or tetrachlorethylene, by (a) adding distillation residue in evaporator, evaporating, condensing and adding in sublimator, (b) fractionating and separating trichloromethane, carbon tetrachloride and tetrachloroethylene, heating, condensing and cooling to obtain hexachloroethane, and (c) refining hexachloroethane, dissolving and adding in crystallization pot, adding crystals into centrifugal filter, collecting filter cake and filtrate, and obtaining filter cake to obtain hexachloroethane.    USE - The method is useful for recycling organic chlorides from distillation residue of methane chloride and/or tetrachloroethylene (claimed).    ADVANTAGE - The method is simple and environmentally-friendly, requires simple device, does not require additional use of solvent and raw material, and provides improved social benefits.    DETAILED DESCRIPTION - Method for recycling organic chlorides from distillation residue of methane chloride and/or tetrachlorethylene, involves (a) adding methane chloride and/or tetrachlorethylene distillation residue in a evaporator, evaporating at 0.01-0.1 MPa and 140-150 degrees C for 30 minutes until there is no liquid to obtain a wet gel, condensing volatile component into liquid, filtering the liquid, and adding in sublimator, (b) fractionating using rectifying system, separating the trichloromethane, carbon tetrachloride and tetrachloroethylene, at the same time heating to 240-250 degrees C using conduction oil sublimator, condensing and opening cooling water, and cooling to obtain hexachloroethane primary product, and (c) refining the primary hexachloroethane using boiler, maintaining low temperature at 45-50 degrees C to completely dissolve hexachloroethane, dissolving obtained solution, adding in crystallization pot, maintaining the temperature and crystallizing at 25 degrees C, adding the obtained crystals into centrifugal filter, collecting filter cake and filtrate, obtaining filter cake to obtain the hexachloroethane, and adding the filtrate into the evaporator for circulating continuously.